MatE 443 - Ferrous Metallurgy Laboratory



Mat E 443 - Laboratory Overview


The laboratory exercises that students perform as a part of this module are intended to supplement the lecture component of ISU MatE 443, Ferrous Metallurgy, and to provide laboratory-based hands-on experiences in various aspects of the microstructure, properties, and performance of steels and cast irons. The laboratory module consists of six independent exercises, which be be completed in student groups or teams.

  • Lab 1: Microstructural Analysis of Steels and Cast Irons
  • Lab 2: Introduction to the Heat Treatment of Steels
  • Lab 3: Quenching and Critical Diameter
  • Lab 4: Tempering of Steels
  • Lab 5: The Jominy End-Quench Test
  • Lab 6: Heat Transfer During Quenching (Computational Exercise)

  • Each team will work independently, except in certain cases where data sharing between teams is required, as indicated by the instructor. Each team will maintain a laboratory logbook, where laboratory activities, observations, results, and analyses are recorded in journal format. Logbooks will be submitted and considered by the instructor as a part of the overall laboratory grade. All logbook pages should be numbered, and all entries should begin with the date, time, name of the person making the entry, and a refernce to the relevant lab exercise. Each team is required to prepare and submit a report for each exercise by the indicated due date. Reports are to be web-based and are to be submitted electronically, as directed by the instructor. The exercises are scheduled in one or two week periods, but lab work is generally "self-scheduled" and teams are welcome to work ahead if desired. However, students are responsible to be sure that the necessary training and instruction is received to ensure that all activities are carrieed out in a safe manner.

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    Mat E 443 - Laboratory Safety


    An objective of this module is to provide a postitive and SAFE environment for students to obtain hands-on laboratory experience, while working with steels and other ferrous alloys. Each student is required to bring his/her safety glasses and to where them in all designated spaces. Sharing of safety glasses is NOT permitted. Students will be given specific instructions for all equipments and activities. Some instructions are available in written or web-based form. Others will be verbal. In any case, it is the students resposnibility to ask questions if any of these instructions are not clearly understood. In addition, it is the students responsibility to notify the instructor or laboratory teaching assistant immediately if any potentially unsafe condition is observed or percieved. Because many students will be sharing space, supplies, and equipment, it is important that all students operate in the most conciencious and courteous manner possible. General cleanliness is imperative for overall lab safety. Laboratory workspace clutter invariably leads to potentially unsafe conditions (and also to sloppy experimental work). At the beginning of the semester, all students will receive instruction regarding laboratory hygiene and maintenance. It is every students responsibiltiy to clean up after/during work, perform necessary equipment cleaning, properly store all tools and lab supplies, properly label and store all material specimens, properly store all chemicals, and properly handle all chemical waste. Note - if everyone does his/her part, then everyone benfits by having a clean, well-functioning laboratory.

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    Mat E 443 - Laboratory Exercises


    The lab exercises and project are listed below, with due dates and links to the full procedures and assignments.
    DATE TITLE REPORT DUE
    8/24 Microstructural Analysis of Steels and Cast Irons 9/7
    9/7 Introduction to the Heat Treatment of Steels 9/21
    9/21 Quenching and Critical Diameter 9/28
    9/28 Tempering of Steels 10/5
    10/5 The Jominy End-Quench Test 10/12
    10/12 Heat Transfer During Quenching 10/19
    10/19 Laboratory Project 11/26

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    Mat E 443 - Laboratory Instructions


    Instructions for selected laboratory equipment is available using the links below. Please keep in mind that there may be supplemental instructions from your instructor.

  • LECO Microhardness Tester
  • LECO Rockwell Hardness Tester
  • Buehler Rockwell Hardness Tester
  • ASM Metallographer's Guide - Intro to Steels and Cast Irons
  • Measurement of ASTM Grain size number
  • LECO Specimen Mounting Press
  • Olympus Microscope and DP12 Camera
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    Mat E 443 - Student Lab Teams (Fall-2007)


    All laboratory exercises will be performed in teams, as indicated below. Each team is required to submit a lab report for each exercise.

    ALLIGATORS
    Fischer
    Sunseri
    Ament
    BISON
    King
    Meyer
    Cleveland
    Rabe
    BONGOS
    Oster
    Czerniak
    Britson
    LEOPARDS
    Sarobol
    Kidd
    Fisher
    OTTERS
    Schmidt
    Wilwert
    Lantz
    Miller
    PRAIRIE DOGS
    Neisen
    Merrick
    Radtke
    SCORPIONS
    Schoenenberger
    Krull
    Muller
    Duzik
    TAPIRS
    Stone
    McPeak
    Zuelke
    Ferguson

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    Mat E 443 - Laboratory Reports

    Each team will be required to submit one laboratory report for each laboratory exercise. All laboratory reports are to be formatted in html and ready for viewing with a standard web browser. As a minimum, reports should include: (i) title, (ii) team name and members, (iii) an introduction with background and motivation, (iv) a statement of objectives, (v) a description of the procedures used, (vi) a results section describing observations and data, (vii) analysis and discussion, (viii) conclusions, (ix) references, and (x) related links. Please use figures and tables effectively, providing interactive links to facilitate understanding. Grading will be based on (i) technical content, (ii) use of English, (iii) effective use of web platform.

    All laboratory reports are to be subbmitted electronically by placing a folder with all html files and supporting files into the "Report Submission Dropbox" folder on the class file server. You will be given the location of this folder in class. Be sure that the submitted folder is clearly labeled with the Lab number, Team name, and year (e.g. Lab2_Tapirs_F07). Submissions must be made by 5pm on the posted dute date. Late reports will be graded for reduced credit (reduced 20% per day). All reports will be posted on the class website for public viewing.

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    Mat E 443 - Laboratory Projects

    Each team is required to complete a laboratory project, where the team will analyze an assigned engineered component, made from a ferrous alloy. The team is expected to (i) review/assess the design/service requirments for the component, (ii) characterize the microstructure (this may require analysis in several locations of the part), (iii) assess the processes used to manufacture the part, (iv) assess the alloy used for the part, (v) give a professional critique of the design, offering alternatives if appropriate, and (v) write a specification for purchasing the material to fabricate the component.

    A short web-based report of part will be submitted by the indicated due date. This should . Clearly state the name of the part. Give a brief summary of what the part is intended to do, and include photographs of the part in the "as received" condition. If necessary, photographs or schematics showing how the part is used in the larger system should be included. From your investigation, include photographs of microstructure and any quantitative results (i.e. phase fraction, composition, hardness profiles, etc.). Based on your analyses and also on any relevant literature, state your best assessment of material and processes used to fabricate the component. In conclusion, include your critique of the design (including material selection and processing).

    In addition to the web-based report, each team will be given 15-20 minutes to present their results in class. The presentations will be held during the last two weeks of the course and are intended to be interactive discussions that will also serve as a semester review.

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